HiME
The first battle with Natsuki and Mikoto
Tate and Takumi's death and Mai's reaction to it (I actually said "Holy shit" during that scene)
Alyssa's death scene and Miyu crying (it broke my heart)
Natsuki being rescued from Nao by Shizuru
Otome
The first scene with Lena
The hiking episode (especially Tomoe and Nina)
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